Ethanone, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-phenyl-

Base Information

Chemical Name:Ethanone, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-phenyl-
CAS No.:103548-04-5
Molecular Formula:C14H22O2Si
Molecular Weight:250.413
Hs Code.:
Mol file:103548-04-5.mol

Synonyms:2-(t-butyldimethylsilyloxy)-acetophenone;α-t-butyldimethylsilyloxy acetophenone;2-(tert-butyl-dimethylsilanyloxy)-1-phenylethanone;α-(tert-butyldimethylsilyloxy)acetophenone;2-(tert-butyldimethylsilyloxy)-1-phenylethanone;2-{[tert-butyl(dimethyl)silyl]oxy}-1-phenylethanone;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanone, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-phenyl-

Chemical Property:

Melting Point:73-74 °C
Boiling Point:294.4±23.0 °C(Predicted)
PSA：26.30000
Density:0.955±0.06 g/cm3(Predicted)
LogP:3.89110

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-phenyl-

There total 7 articles about Ethanone, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 582-24-1
1-phenyl-2-hydroxyethanone

: 103548-04-5
2-(tert-butyldimethylsilanyloxy)-1-phenylethan-1-one

Guidance literature:: 1-phenyl-2-hydroxyethanone; With 1H-imidazole; In dichloromethane; at 20 ℃; for 0.166667h;

tert-butyldimethylsilyl chloride; at 20 ℃; for 5h;
DOI:10.1021/acs.orglett.0c02117

Reference yield: 93.0%

: 66324-10-5
tert-butyldimethyl(1-phenylvinyloxy)silane

: 103548-04-5
2-(tert-butyldimethylsilanyloxy)-1-phenylethan-1-one

Guidance literature:: With oxygen; isobutyraldehyde; bis(3-methyl-2,4-pentanedionato)nickel(II); In 1,2-dichloro-ethane; for 4h; Ambient temperature;

Reference yield: 93.0%

: 71009-09-1
2-(tert-butyldimethylsilyl)oxy-1-phenylethanol

: 103548-04-5
2-(tert-butyldimethylsilanyloxy)-1-phenylethan-1-one

Guidance literature:: With chlorine-triphenylphosphine; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃; for 3.25h; Further Variations:; Reagents; Temperatures; Product distribution;
DOI:10.1016/S0040-4039(02)02004-X