toluene-4-sulfonic acid 5-{[3-(anthracen-9-ylmethyl-tert-butoxycarbonyl-amino)-propyl]-tert-butoxycarbonyl-amino}-pentyl ester

Base Information

• Chemical Name: toluene-4-sulfonic acid 5-{[3-(anthracen-9-ylmethyl-tert-butoxycarbonyl-amino)-propyl]-tert-butoxycarbonyl-amino}-pentyl ester
• CAS No.: 1027032-58-1
• Molecular Formula: C₄₀H₅₂N₂O₇S
• Molecular Weight: 704.928
• Mol file: 1027032-58-1.mol

Synonyms:

Chemical Property of toluene-4-sulfonic acid 5-{[3-(anthracen-9-ylmethyl-tert-butoxycarbonyl-amino)-propyl]-tert-butoxycarbonyl-amino}-pentyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of toluene-4-sulfonic acid 5-{[3-(anthracen-9-ylmethyl-tert-butoxycarbonyl-amino)-propyl]-tert-butoxycarbonyl-amino}-pentyl ester

There total 3 articles about toluene-4-sulfonic acid 5-{[3-(anthracen-9-ylmethyl-tert-butoxycarbonyl-amino)-propyl]-tert-butoxycarbonyl-amino}-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-hydroxypentylamine (2508-29-4) → toluene-4-sulfonic acid 5-{[3-(anthracen-9-ylmethyl-tert-butoxycarbonyl-amino)-propyl]-tert-butoxycarbonyl-amino}-pentyl ester (1027032-58-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent / acetonitrile / 75 °C

2: pyridine / methanol / 0 - 20 °C

3: pyridine / 1 h

With pyridine; In methanol; acetonitrile;

DOI:10.1021/jm020598g

Reference yield:

anthracen-9-ylmethyl[3-(5-hydroxypentylamino)propyl]carbamic acid tert-butyl ester (569372-63-0) → toluene-4-sulfonic acid 5-{[3-(anthracen-9-ylmethyl-tert-butoxycarbonyl-amino)-propyl]-tert-butoxycarbonyl-amino}-pentyl ester (1027032-58-1)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / methanol / 0 - 20 °C

2: pyridine / 1 h

With pyridine; In methanol;

DOI:10.1021/jm020598g

Reference yield:

4-methylbenzenesulfonic acid 3-[(anthracen-9-ylmethyl)(tert-butoxycarbonyl)amino]propyl ester (561300-94-5) → toluene-4-sulfonic acid 5-{[3-(anthracen-9-ylmethyl-tert-butoxycarbonyl-amino)-propyl]-tert-butoxycarbonyl-amino}-pentyl ester (1027032-58-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent / acetonitrile / 75 °C

2: pyridine / methanol / 0 - 20 °C

3: pyridine / 1 h

With pyridine; In methanol; acetonitrile;

DOI:10.1021/jm020598g

upstream raw materials:

5-hydroxypentylamine

4-methylbenzenesulfonic acid 3-[(anthracen-9-ylmethyl)(tert-butoxycarbonyl)amino]propyl ester

anthracen-9-ylmethyl[3-(5-hydroxypentylamino)propyl]carbamic acid tert-butyl ester