N-(+)-(3R)-menthyloxycarbonyl-N'-morpholinothiourea

Base Information

Chemical Name:N-(+)-(3R)-menthyloxycarbonyl-N'-morpholinothiourea
CAS No.:331823-17-7
Molecular Formula:C₁₆H₂₈N₂O₃S
Molecular Weight:328.476
Hs Code.:

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Chemical Property of N-(+)-(3R)-menthyloxycarbonyl-N'-morpholinothiourea

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Technology Process of N-(+)-(3R)-menthyloxycarbonyl-N'-morpholinothiourea

There total 1 articles about N-(+)-(3R)-menthyloxycarbonyl-N'-morpholinothiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 110-91-8,99108-56-2
morpholine

: 7635-54-3,7635-53-2
(+)-(1S,2R,5S)-menthylchloroformate

: 333-20-0
potassium thioacyanate

: 331823-17-7
N-(+)-(3R)-menthyloxycarbonyl-N'-morpholinothiourea

Guidance literature:: (+)-(1S,2R,5S)-menthylchloroformate; potassium thioacyanate; In acetone; for 2h; Heating;

morpholine; In acetone; for 2h; Further stages.; Heating;
DOI:10.1039/b007589m

Reference yield: 80.0%

: 75992-73-3,25794-47-2,30729-25-0,15274-33-6,22840-91-1,14568-13-9
cis-dichlorobis(dimethylsulfoxide)platinum(II)

: 331823-17-7
N-(+)-(3R)-menthyloxycarbonyl-N'-morpholinothiourea

: cis-(S,S)-[PtCl(O(CH₂)4NCSNCOC₆H₉(CH₃)((CH₃)2CH))(DMSO)]

Guidance literature:: With NaCH₃COO; In water; dimethyl sulfoxide; acetonitrile; addn. dropwise of soln. of (OC4H8NCSNCOOC6H9(CH3)((CH3)2CH) (1 equiv.) in CH3CN to soln. of PtCl2(DMSO)2 (1 equiv.) in CH3CN-DMSO (1:1), addn. of NaCH3COO in water, stirring at room temp. for 3 days; addn. of water, cooling at 4°C overnight, filtration, washing with water, C2H5OH and drying in vac. over silica gel; elem. anal.;
DOI:10.1039/b007589m