2-(4-methoxyphenyl)-1,3-dimethylhexahydropyrimidine

Base Information

• Chemical Name: 2-(4-methoxyphenyl)-1,3-dimethylhexahydropyrimidine
• CAS No.: 57648-66-5
• Molecular Formula: C₁₃H₂₀N₂O
• Molecular Weight: 220.315
• Mol file: 57648-66-5.mol

Synonyms:

Chemical Property of 2-(4-methoxyphenyl)-1,3-dimethylhexahydropyrimidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-methoxyphenyl)-1,3-dimethylhexahydropyrimidine

There total 2 articles about 2-(4-methoxyphenyl)-1,3-dimethylhexahydropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-methoxy-benzaldehyde (123-11-5) + 1,3-bis(methylamino)propane (111-33-1) → 2-(4-methoxyphenyl)-1,3-dimethylhexahydropyrimidine (57648-66-5)

Guidance literature:

With ammonium chloride; for 1h; Dean-Stark; Reflux; Green chemistry;

DOI:10.1039/c5gc00465a

Reference yield:

→ 2-(4-methoxyphenyl)-1,3-dimethylhexahydropyrimidine (57648-66-5)

Guidance literature:

/BRN= 773668/, /BRN= 471382/;

DOI:10.1055/s-1975-23874

upstream raw materials:

4-methoxy-benzaldehyde

1,3-bis(methylamino)propane