Boc-ΔOrn(Cbz)-OMe

Base Information

Chemical Name:Boc-ΔOrn(Cbz)-OMe
CAS No.:114684-76-3
Molecular Formula:C₁₉H₂₆N₂O₆
Molecular Weight:378.425
Hs Code.:

Synonyms:

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Chemical Property of Boc-ΔOrn(Cbz)-OMe

Chemical Property:

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Technology Process of Boc-ΔOrn(Cbz)-OMe

There total 5 articles about Boc-ΔOrn(Cbz)-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65564-05-8
3-[(benzyloxycarbonyl)amino]propanal

: 114684-76-3
Boc-ΔOrn(Cbz)-OMe

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / t-BuOK / CH₂Cl₂ / -60 deg C 1 h and room temp 3 h

2: 80 percent / 1 M LiOH / 3 h / Ambient temperature

3: 93 percent / SOCl₂ / diethyl ether

4: 2.) N-methylmorpholin

With 4-methyl-morpholine; lithium hydroxide; thionyl chloride; potassium tert-butylate; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)96397-4

Reference yield:

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 114684-76-3
Boc-ΔOrn(Cbz)-OMe

Guidance literature:: Multi-step reaction with 5 steps

1: CrO₃ and further five oxidizing reagents / pyridine / 1.5 h

2: 90 percent / t-BuOK / CH₂Cl₂ / -60 deg C 1 h and room temp 3 h

3: 80 percent / 1 M LiOH / 3 h / Ambient temperature

4: 93 percent / SOCl₂ / diethyl ether

5: 2.) N-methylmorpholin

With 4-methyl-morpholine; chromium(VI) oxide; lithium hydroxide; thionyl chloride; potassium tert-butylate; In pyridine; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)96397-4

Reference yield:

: 54755-77-0
N-benzyloxycarbonyl-3-aminopropionic acid methyl ester

: 114684-76-3
Boc-ΔOrn(Cbz)-OMe

Guidance literature:: Multi-step reaction with 6 steps

1: NaBH₄ / LiAlH₄

2: CrO₃ and further five oxidizing reagents / pyridine / 1.5 h

3: 90 percent / t-BuOK / CH₂Cl₂ / -60 deg C 1 h and room temp 3 h

4: 80 percent / 1 M LiOH / 3 h / Ambient temperature

5: 93 percent / SOCl₂ / diethyl ether

6: 2.) N-methylmorpholin

With 4-methyl-morpholine; chromium(VI) oxide; lithium hydroxide; sodium tetrahydroborate; thionyl chloride; potassium tert-butylate; In pyridine; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)96397-4