Carbamic acid, [3-(phenylmethyl)-2-pyridinyl]-, ethyl ester

Base Information

Chemical Name:Carbamic acid, [3-(phenylmethyl)-2-pyridinyl]-, ethyl ester
CAS No.:153230-22-9
Molecular Formula:C₁₅H₁₆N₂O₂
Molecular Weight:256.304
Hs Code.:
DSSTox Substance ID:DTXSID501190998

Synonyms:Carbamic acid, [3-(phenylmethyl)-2-pyridinyl]-, ethyl ester;DTXSID501190998;153230-22-9

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [3-(phenylmethyl)-2-pyridinyl]-, ethyl ester

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:256.121177757
Heavy Atom Count:19
Complexity:277

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)NC1=C(C=CC=N1)CC2=CC=CC=C2

Technology Process of Carbamic acid, [3-(phenylmethyl)-2-pyridinyl]-, ethyl ester

There total 2 articles about Carbamic acid, [3-(phenylmethyl)-2-pyridinyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 541-41-3
chloroformic acid ethyl ester

: 130277-16-6
2-amino-3-benzylpyridine

: 153230-22-9
N-(3-Benzyl-2-pyridyl)carbamidsaeureethylester

Guidance literature:: With pyridine; for 3h; 1.) 0 deg C, 15 min, 2.) 50 deg C, 12 h;
DOI:10.1002/ardp.19933261114

Reference yield:

: 153230-23-0
1-(3-Benzyl-2-pyridylaminocarbonyl)-4-methyl-piperazin

: 153230-22-9
N-(3-Benzyl-2-pyridyl)carbamidsaeureethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / PPA, POCl₃ / 1.) 145-150 deg C, 3 h, 2.) 175-180 deg C, 1 h

2: 50 percent / pyridine / 3 h / 1.) 0 deg C, 15 min, 2.) 50 deg C, 12 h

With pyridine; trichlorophosphate;
DOI:10.1002/ardp.19933261114