chromium(III) (acetate)tetraphenylporphyrinate

Base Information

Chemical Name:chromium(III) (acetate)tetraphenylporphyrinate
CAS No.:82025-66-9
Molecular Formula:C₄₆H₃₁CrN₄O₂
Molecular Weight:723.774
Hs Code.:

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Chemical Property of chromium(III) (acetate)tetraphenylporphyrinate

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Technology Process of chromium(III) (acetate)tetraphenylporphyrinate

There total 2 articles about chromium(III) (acetate)tetraphenylporphyrinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: chromium(II) acetate

: 82025-66-9
chromium(III) (acetate)tetraphenylporphyrinate

Guidance literature:: With air; In N,N-dimethyl-formamide; the porphine is dissolved in boiling DMF, addn. of the Cr salt, boile in presence of the oxygen of air; addn. of CHCl3, evapd., residue is dissolved in a minimal quantity of CHCl3, chromy., evapd., dried at 373 K for 2 h, elem. anal.;

Reference yield: 50.0%

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: 1066-30-4
chromium(lll) acetate

: 82025-66-9
chromium(III) (acetate)tetraphenylporphyrinate

Guidance literature:: In further solvent(s); mixt. of the phosphine and Cr(III) acetate in phenol heated at reflux for 6 h; cooled, dissolved in CHCl3, washed with warm H2O, passed through Al2O3 column, solvent removed under vac.; elem. anal.;
DOI:10.1023/A:1021630228084