TiCl₃(2,6-i-Pr₂C₆H₃O)

Base Information

Chemical Name:TiCl₃(2,6-i-Pr₂C₆H₃O)
CAS No.:151041-51-9
Molecular Formula:C₁₂H₁₇Cl₃OTi
Molecular Weight:331.505
Hs Code.:

TiCl<sub>3</sub>(2,6-i-Pr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>O)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of TiCl₃(2,6-i-Pr₂C₆H₃O)

Chemical Property:

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Technology Process of TiCl₃(2,6-i-Pr₂C₆H₃O)

There total 1 articles about TiCl₃(2,6-i-Pr₂C₆H₃O) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2078-54-8
2,6-diisopropylphenol

: 7550-45-0
titanium tetrachloride

: 151041-51-9
TiCl₃(2,6-i-Pr₂C₆H₃O)

Guidance literature:: In toluene; byproducts: HCl; under N2; 2,6-diisopropylphenol in toluene added to TiCl4 (molar ratio 1:1) in toluene; refluxed for 12 h; filtered; solvent removed; solidified on gentle heating (water bath 60-70°C) under vac. for several h; elem. anal.;
DOI:10.1039/a908435e

Reference yield:

: 1134-35-6
4,4'-dimethyl-2,2'-bipyridines

: 151041-51-9
TiCl₃(2,6-i-Pr₂C₆H₃O)

: 263546-99-2
mer-trichloro(4,4'-dimethyl-2,2'-bipyridyl)mono(2,6-diisopropylphenoxide)titanium(IV)

Guidance literature:: In dichloromethane; under N2; 1 equiv. of ligand in CH2Cl2 added to stirred soln. of Ti complex in CH2Cl2; stirred for 2 h; filtered; solvent removed; stood under light petroleum for 2 d; filtered; elem. anal.;
DOI:10.1039/a908435e

Reference yield:

: 1134-35-6
4,4'-dimethyl-2,2'-bipyridines

: 151041-51-9
TiCl₃(2,6-i-Pr₂C₆H₃O)

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: mer-trichloro(4,4'-dimethyl-2,2'-bipyridyl)mono(2,6-diisopropylphenoxide)titanium(IV)*0.83(benzene)

Guidance literature:: In benzene; under N2; 1 equiv. of ligand in benzene added rapidly to soln. of Ti complex in light petroleum; stirred for 1 h; filtered; solid washed with light petroleum; dried in vac. for 2 h; elem. anal.;
DOI:10.1039/a908435e