DL-Phenylalanine, N-(4-methoxybenzoyl)-

Base Information

Chemical Name:DL-Phenylalanine, N-(4-methoxybenzoyl)-
CAS No.:103678-74-6
Molecular Formula:C17H17NO4
Molecular Weight:299.326
Hs Code.:
Mol file:103678-74-6.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of DL-Phenylalanine, N-(4-methoxybenzoyl)-

Chemical Property:

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Technology Process of DL-Phenylalanine, N-(4-methoxybenzoyl)-

There total 15 articles about DL-Phenylalanine, N-(4-methoxybenzoyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: Phe-Wang resin

: 696-62-8
para-iodoanisole

: 18414-58-9
diphenylmethylsilanecarboxylic acid

: 103678-74-6,105746-31-4,59490-31-2
(4-methoxybenzoyl)-L-phenylalanine

Guidance literature:: Phe-Wang resin; para-iodoanisole; diphenylmethylsilanecarboxylic acid; With potassium fluoride; C₃₉H₃₂OP₂*C₁₃H₁₂N^(1-)*Pd⁽²⁺⁾*CH₃O₃S^(1-); triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 15h; wang polystyrene resin Sealed tube; Inert atmosphere;

With triethylsilane; trifluoroacetic acid; In water; at 20 ℃; for 2h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.7b01068

Reference yield: 35.0%

: C₁₇H₁₇N₂O₃Pol

: 1586780-57-5
α-[(4-methoxybenzoyl)amino]benzenepropanamide

: 103678-74-6,105746-31-4,59490-31-2
(4-methoxybenzoyl)-L-phenylalanine

Guidance literature:: With water; trifluoroacetic acid; at 20 ℃; for 5.5h; Rink amide MBHA resin
DOI:10.1021/jo500273f

Reference yield:

: 150-30-1,25191-15-5,658-69-5,67675-33-6
Phenylalanine

: 100-07-2
4-methoxy-benzoyl chloride

: 103678-74-6
N-(4-methoxybenzoyl)-phenylalanine

Guidance literature:: Phenylalanine; With sodium hydroxide; In dichloromethane; water; at 0 ℃;

4-methoxy-benzoyl chloride; In dichloromethane; water; at 0 - 20 ℃; for 3h;
DOI:10.1002/ejoc.201403158