2-diphenylmethylsilylethyl dithiophophorodichloridate

Base Information

• Chemical Name: 2-diphenylmethylsilylethyl dithiophophorodichloridate
• CAS No.: 233757-88-5
• Molecular Formula: C₁₅H₁₇Cl₂PS₂Si
• Molecular Weight: 391.397
• Mol file: 233757-88-5.mol

Synonyms:

Chemical Property of 2-diphenylmethylsilylethyl dithiophophorodichloridate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-diphenylmethylsilylethyl dithiophophorodichloridate

There total 2 articles about 2-diphenylmethylsilylethyl dithiophophorodichloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenylmethylsilylethylethanol (40438-48-0) → 2-diphenylmethylsilylethyl dithiophophorodichloridate (233757-88-5)

Guidance literature:

Multi-step reaction with 2 steps

1: PCl₃ / diethyl ether / 2 h / 0 °C

2: PSCl₃; S₈; charcoal / 8 h / Heating

With sulfur; pyrographite; trichlorophosphate; phosphorus trichloride; In diethyl ether; 1: Substitution / 2: Substitution;

DOI:10.1080/07328319908044666

Reference yield:

C15H17Cl2OPSi (289698-26-6) → 2-diphenylmethylsilylethyl dithiophophorodichloridate (233757-88-5)

Guidance literature:

With sulfur; pyrographite; trichlorophosphate; for 8h; Heating;

DOI:10.1080/07328319908044666

Reference yield:

6-trifluoromethyl-1-hydroxybenzotriazole (26198-21-0) + 2-diphenylmethylsilylethyl dithiophophorodichloridate (233757-88-5) → O,O-bis(6-trifluoromethylbenzotriazole-1-yl) S-2-diphenylmethylsilyl-ethyl dithiophophotriester (289698-33-5)

Guidance literature:

With pyridine; In 1,4-dioxane; at 20 ℃; for 1h;

DOI:10.1080/07328319908044666

upstream raw materials:

C₁₅H₁₇Cl₂OPSi

diphenylmethylsilylethylethanol

Downstream raw materials:

O,O-bis(6-trifluoromethylbenzotriazole-1-yl) S-2-diphenylmethylsilyl-ethyl dithiophophotriester