Technology Process of N-(Diphenylphosphinoyl)-S-benzoylthiohydroxylamine
There total 7 articles about N-(Diphenylphosphinoyl)-S-benzoylthiohydroxylamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sulfur / toluene / 4.5 h / Heating
2: triethylamine / dichloromethane / 1.) ice-cooled, 15 min, 2.) r.t., overnight
3: methanol / 1.5 h
4: triethylamine / dichloromethane / 0.08 h
5: dichloromethane
With
methanol; sulfur; triethylamine;
In
dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 1.) ice-cooled, 15 min, 2.) r.t., overnight
2: methanol / 1.5 h
3: triethylamine / dichloromethane / 0.08 h
4: dichloromethane
With
methanol; triethylamine;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 0.08 h
2: dichloromethane
With
triethylamine;
In
dichloromethane;
