Benzene, 1-[3-[(2-methyl-3-butynyl)oxy]propyl]-4-(phenylmethoxy)-

Base Information

Chemical Name:Benzene, 1-[3-[(2-methyl-3-butynyl)oxy]propyl]-4-(phenylmethoxy)-
CAS No.:103768-06-5
Molecular Formula:C21H24O2
Molecular Weight:308.42
Hs Code.:
Mol file:103768-06-5.mol

Synonyms:

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Chemical Property of Benzene, 1-[3-[(2-methyl-3-butynyl)oxy]propyl]-4-(phenylmethoxy)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzene, 1-[3-[(2-methyl-3-butynyl)oxy]propyl]-4-(phenylmethoxy)-

There total 3 articles about Benzene, 1-[3-[(2-methyl-3-butynyl)oxy]propyl]-4-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-97-3
4-hydroxyphenylpropionic acid

: 103768-06-5
1-Benzyloxy-4-[3-(2-methyl-but-3-ynyloxy)-propyl]-benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium hydride; 2.) HMPT / 2.) tetrabutylammonium iodide / 1.) THF, 3 h; 2.) THF, reflux, 15 h

2: 95 percent / lithium-aluminium hydride / diethyl ether / 0.25 h

3: HCl / CH₂Cl₂ / 0.03 h / -10 °C

4: aluminium / tetrahydrofuran / 3 h / 60 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; sodium hydride; aluminium; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 113647-42-0,18668-72-9
3-Bromo-but-1-yne

: 104211-82-7
1-Benzyloxy-4-(3-chloromethoxy-propyl)-benzene

: 103768-06-5
1-Benzyloxy-4-[3-(2-methyl-but-3-ynyloxy)-propyl]-benzene

Guidance literature:: In tetrahydrofuran; reaction with the aluminium derivative obtained from the propargylic bromide;
DOI:10.1016/S0040-4039(00)98271-6

Reference yield:

: 58608-97-2
3-(4-benzyloxyphenyl)propionic acid benzyl ester

: 103768-06-5
1-Benzyloxy-4-[3-(2-methyl-but-3-ynyloxy)-propyl]-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / lithium-aluminium hydride / diethyl ether / 0.25 h

2: HCl / CH₂Cl₂ / 0.03 h / -10 °C

3: aluminium / tetrahydrofuran / 3 h / 60 °C

With hydrogenchloride; lithium aluminium tetrahydride; aluminium; In tetrahydrofuran; diethyl ether; dichloromethane;