N,N-dimethyl-4-(4-oxopentyl)benzamide

Base Information

Chemical Name:N,N-dimethyl-4-(4-oxopentyl)benzamide
CAS No.:615581-70-9
Molecular Formula:C₁₄H₁₉NO₂
Molecular Weight:233.31
Hs Code.:

Synonyms:

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Chemical Property of N,N-dimethyl-4-(4-oxopentyl)benzamide

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Technology Process of N,N-dimethyl-4-(4-oxopentyl)benzamide

There total 8 articles about N,N-dimethyl-4-(4-oxopentyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86608-70-0
2-(1,3-dioxolan-2-yl)ethyl(triphenyl)phosphonium bromide

: 615581-70-9
N,N-dimethyl-4-(4-oxopentyl)benzamide

Guidance literature:: Multi-step reaction with 8 steps

1.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

1.2: 90 percent / tetrahydrofuran / 1 h / 0 °C

2.1: H₂ / Pd/C / methanol / 0.5 h / 20 °C / 760 Torr

3.1: 99 percent / PPTS / acetone; H₂O / 12 h / Heating

4.1: 56 percent / tetrahydrofuran / 1 h / -40 °C

5.1: 88 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.5 h / 20 °C

6.1: 91 percent / LiOH*H₂O / methanol; H₂O / 0 - 20 °C

7.1: SOCl₂ / CH₂Cl₂; dimethylformamide / 2 h / 20 °C

8.1: H₂O; CH₂Cl₂; dimethylformamide / 0 °C

With lithium hydroxide; thionyl chloride; hydrogen; pyridinium p-toluenesulfonate; sodium hydride; Dess-Martin periodane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; 1.2: Wittig olefination;
DOI:10.1021/jo034767w

Reference yield:

: 667909-36-6
4-((E)-3-[1,3]Dioxolan-2-yl-propenyl)-benzoic acid methyl ester

: 615581-70-9
N,N-dimethyl-4-(4-oxopentyl)benzamide

Guidance literature:: Multi-step reaction with 7 steps

1: H₂ / Pd/C / methanol / 0.5 h / 20 °C / 760 Torr

2: 99 percent / PPTS / acetone; H₂O / 12 h / Heating

3: 56 percent / tetrahydrofuran / 1 h / -40 °C

4: 88 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.5 h / 20 °C

5: 91 percent / LiOH*H₂O / methanol; H₂O / 0 - 20 °C

6: SOCl₂ / CH₂Cl₂; dimethylformamide / 2 h / 20 °C

7: H₂O; CH₂Cl₂; dimethylformamide / 0 °C

With lithium hydroxide; thionyl chloride; hydrogen; pyridinium p-toluenesulfonate; Dess-Martin periodane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo034767w

Reference yield:

: 106200-41-3
4-(4-carbomethoxyphenyl)butanal

: 615581-70-9
N,N-dimethyl-4-(4-oxopentyl)benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: 56 percent / tetrahydrofuran / 1 h / -40 °C

2: 88 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.5 h / 20 °C

3: 91 percent / LiOH*H₂O / methanol; H₂O / 0 - 20 °C

4: SOCl₂ / CH₂Cl₂; dimethylformamide / 2 h / 20 °C

5: H₂O; CH₂Cl₂; dimethylformamide / 0 °C

With lithium hydroxide; thionyl chloride; Dess-Martin periodane; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo034767w