Quinoline, 2,3,4-triphenyl-

Base Information

• Chemical Name: Quinoline, 2,3,4-triphenyl-
• CAS No.: 10380-73-1
• Molecular Formula: C27H19N
• Molecular Weight: 357.455
• Mol file: 10380-73-1.mol

Synonyms:

Chemical Property of Quinoline, 2,3,4-triphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Quinoline, 2,3,4-triphenyl-

There total 19 articles about Quinoline, 2,3,4-triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.1%

diphenyl acetylene (501-65-5) + (2-aminophenyl)(phenyl)methanone (2835-77-0) → 2,3,4-triphenyl quinoline (10380-73-1)

Guidance literature:

With 18-crown-6 ether; trifluorormethanesulfonic acid; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane; In toluene; acetonitrile; at 105 ℃; for 11h; Reagent/catalyst; Solvent; Sealed tube;

Reference yield: 97.0%

Benzophenone oxime (574-66-3) + diphenyl acetylene (501-65-5) → 2,3,4-triphenyl quinoline (10380-73-1)

Guidance literature:

With trifluoromethylsulfonic anhydride; In 1,2-dichloro-ethane; at 0 - 80 ℃; for 12h;

DOI:10.1002/adsc.201801724

Reference yield: 92.0%

3-iodo-2,4-diphenylquinoline + phenylboronic acid (98-80-6) → 2,3,4-triphenyl quinoline (10380-73-1)

Guidance literature:

With palladium diacetate; sodium carbonate; In water; N,N-dimethyl-formamide; at 100 ℃; for 4h; Inert atmosphere; Sealed vessel;

DOI:10.1021/ol2007154

upstream raw materials:

diphenyl acetylene

(E)-N-benzylidenebenzenamine

phenyl benzyl ketone

(2-aminophenyl)(phenyl)methanone

Downstream raw materials:

1-Ethyl-3,4-diphenyl-1H-quinolin-2-one