C₂₅H₄₆O₇S₂Si

Base Information

Chemical Name:C₂₅H₄₆O₇S₂Si
CAS No.:1316846-70-4
Molecular Formula:C₂₅H₄₆O₇S₂Si
Molecular Weight:550.854
Hs Code.:

C<sub>25</sub>H<sub>46</sub>O<sub>7</sub>S<sub>2</sub>Si

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Chemical Property of C₂₅H₄₆O₇S₂Si

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Technology Process of C₂₅H₄₆O₇S₂Si

There total 10 articles about C₂₅H₄₆O₇S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 624-92-0
Dimethyldisulphide

: 1316846-69-1
C₂₃H₄₀O₈Si

: 1316846-70-4
C₂₅H₄₆O₇S₂Si

Guidance literature:: With tributylphosphine; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: C₃₁H₄₅F₃O₉SSi

: 1316846-70-4
C₂₅H₄₆O₇S₂Si

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / dichloromethane; water / 0.33 h / 0 °C / Inert atmosphere

2: tributylphosphine / 0 - 20 °C / Inert atmosphere

With tributylphosphine; sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: C₁₄H₁₈O₄

: 1316846-70-4
C₂₅H₄₆O₇S₂Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.5 h / -40 °C

1.2: 1 h / 0 °C

2.1: zinc(II) chloride / tetrahydrofuran / 0.25 h / 20 °C

2.2: 2.17 h / -78 °C

2.3: -78 - 20 °C

3.1: N-Bromosuccinimide; water / toluene / 0.25 h / 20 °C

4.1: potassium carbonate / acetonitrile / 8.25 h / 0 - 20 °C

5.1: 1H-imidazole / dichloromethane / 1 h / 20 °C

6.1: boron trifluoride diethyl etherate / diethyl ether; dichloromethane / 4 h / -78 - 0 °C

6.2: 1 h / 0 - 20 °C

7.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C

8.1: triethylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

9.1: sodium hydrogencarbonate / dichloromethane; water / 0.33 h / 0 °C / Inert atmosphere

10.1: tributylphosphine / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; dmap; N-Bromosuccinimide; tributylphosphine; boron trifluoride diethyl etherate; water; sodium hydrogencarbonate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; toluene; acetonitrile; 8.1: Pummerer reaction;