{Ru(CO)2Cl₂(P(C₆H₅)(CH₃)2)2}

Base Information

Chemical Name:{Ru(CO)2Cl₂(P(C₆H₅)(CH₃)2)2}
CAS No.:17141-01-4
Molecular Formula:C₁₈H₂₂Cl₂O₂P₂Ru
Molecular Weight:504.295
Hs Code.:

{Ru(CO)2Cl<sub>2</sub>(P(C<sub>6</sub>H<sub>5</sub>)(CH<sub>3</sub>)2)2}

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Chemical Property of {Ru(CO)2Cl₂(P(C₆H₅)(CH₃)2)2}

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Technology Process of {Ru(CO)2Cl₂(P(C₆H₅)(CH₃)2)2}

There total 16 articles about {Ru(CO)2Cl₂(P(C₆H₅)(CH₃)2)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 672-66-2
Dimethyl(phenyl)phosphine

: 17141-01-4,17141-04-7,25165-53-1,60426-65-5
cct-(PhMe₂P)2Ru(II)(CO)2Cl₂

Guidance literature:: With carbon monoxide; In 2-methoxy-ethanol; bubbling of CO through a refluxing soln. of RuCl3*3H2O (2-methoxyethanol, 5 h), addn. of a soln. of 2 equivs. PhMe2P in 2-methoxyethanol, refluxing (21 h); drying (vac.), trituration of resulting oil with abs. ethanol, filtration of resulting powder, washing (ethanol), drying (vac., overnight); elem. anal.;

Reference yield: 70.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 201230-82-2
carbon monoxide

: 672-66-2
Dimethyl(phenyl)phosphine

: 2Ru⁽²⁺⁾*4Cl^(1-)*4CO*2P(CH₃)2(C₆H₅) = [Ru₂Cl₄(CO)4(P(CH₃)2C₆H₅)2]

: 17141-01-4,17141-04-7,25165-53-1,60426-65-5
cct-(PhMe₂P)2Ru(II)(CO)2Cl₂

Guidance literature:: In 2-methoxy-ethanol; (inert atmosphere); passing CO through a refluxing soln. of RuCl3*3H2O in 2-methoxyethanol for ca. 5 h, addn. of PMe2Ph, redn. of CO flow with further heating for 12 h; solvent removal (reduced pressure), addn. of acetone, filtration, addn. of EtOH to the filtrate, concn. under a stream of N2; elem. anal.;

Reference yield: 66.0%

: 17141-01-4,17141-04-7,25165-53-1,60426-65-5
all-trans-[Ru(CO)2(PMe₂Ph)Cl₂]

: 593-74-8
dimethylmercury

: 17141-01-4,17141-04-7,25165-53-1,60426-65-5
cct-(PhMe₂P)2Ru(II)(CO)2Cl₂

: [RuCl(CO)2(CH₃)(P(CH₃)2C₆H₅)2]

Guidance literature:: In acetone; N2-atmosphere; excess HgMe2, 313 K, 4 h; solvent removal (reduced pressure), chromy. (Al2O3, CHCl3), recrystn. (light petroleum); elem. anal.;
DOI:10.1039/DT9760000961