Isopropyldiphenylgermane

Base Information

• Chemical Name: Isopropyldiphenylgermane
• CAS No.: 100184-64-3
• Molecular Formula: C₁₅H₁₈Ge
• Molecular Weight: 270.898
• Mol file: 100184-64-3.mol

Synonyms:

Chemical Property of Isopropyldiphenylgermane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Isopropyldiphenylgermane

There total 3 articles about Isopropyldiphenylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.8%

diphenylgermylenedipotassium (100184-59-6) + isopropyl chloride (75-29-6) → (C6H5)2Ge(CH(CH3)2)2 + diphenylgermane (1675-58-7) + Isopropyldiphenylgermane (100184-64-3)

Guidance literature:

With water; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; soln. of Ph2GeK2 in HMPA/THF added to i-PrCl, stirred at room temp. for30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;

DOI:10.1246/bcsj.58.1443

Reference yield: 82.8%

isopropyl chloride (75-29-6) + (diphenylgermylene)dipotassium → Isopropyldiphenylgermane (100184-64-3)

Guidance literature:

In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; for 0.5h; Product distribution; Ambient temperature;

DOI:10.1246/bcsj.58.1443

Reference yield:

isopropyl chloride (75-29-6) + diphenyldibromogermane (1080-42-8) → Isopropyldiphenylgermane (100184-64-3)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1.) ether, benzene, 2.) toluene, reflux, 7 h;;

DOI:10.1246/bcsj.58.1443

upstream raw materials:

isopropyl chloride

diphenyldibromogermane

diphenylgermylenedipotassium