[2,6-bis((dimethylamino)methyl)phenyl]dimethyltin chloride

Base Information

Chemical Name:[2,6-bis((dimethylamino)methyl)phenyl]dimethyltin chloride
CAS No.:115092-11-0
Molecular Formula:C₁₄H₂₅N₂Sn*Cl
Molecular Weight:375.529
Hs Code.:

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Chemical Property of [2,6-bis((dimethylamino)methyl)phenyl]dimethyltin chloride

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Technology Process of [2,6-bis((dimethylamino)methyl)phenyl]dimethyltin chloride

There total 1 articles about [2,6-bis((dimethylamino)methyl)phenyl]dimethyltin chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114762-89-9
Ir{C₆H₃(CH₂NMe₂)-2-(CH₂NMe₂)-6}(COD)

: 2767-47-7
dimethyltin dibromide

: 12245-73-7
{IrBr(COD)}2

: 63400-16-8
{m-(Me₂(H)NCH₂)2C₆H₄}Cl₂

: 115092-11-0
(SnMe₂{C₆H₃(CH₂NMe₂)2-2,6})Cl

Guidance literature:: In benzene; instant decomposition under N2-atmosphere; filtration, adding 1N HCl, hydrochloride isolated from water layer, identification: 1H-NMR;
DOI:10.1021/ja00224a021

Reference yield: 75.0%

: 115092-11-0
[2,6-bis((dimethylamino)methyl)phenyl]dimethyltin chloride

: 563-63-3
silver(I) acetate

: [2,6-bis((dimethylamino)methyl)phenyl]dimethyltin acetate

Guidance literature:: In dichloromethane; byproducts: AgCl; (Ar atm.; Schlenk) CH3CO2Ag in CH2Cl2 was added dropwise to a stirred soln. of Sn-compound in CH2Cl2, stirred for 5 days at room temp.; filtered, evapd. in vac., the residue as washed with pentane; elem. anal.;
DOI:10.1021/om050549c