Technology Process of C48H55N4O17P
There total 6 articles about C48H55N4O17P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-methyl-1H-imidazole; triisopropylbenzenesulfonyl chloride;
In
pyridine;
for 0.5h;
DOI:10.1007/BF02786343
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dicyclohexylcarbodiimide / diethyl ether / 3 h / 20 °C
1.2: N-methylimidazole / pyridine / 0.5 h
2.1: 0.22 g / acetic acid; H2O / 2 h / 40 °C
3.1: 75 percent / triisopropylbenzenesulfonyl chloride; M-methylimidazole / pyridine
4.1: 85 percent / tetrabutylammonium fluoride / pyridine; H2O / 5 h / 50 °C / pH 7.0
5.1: 70 percent / triisopropylbenzenesulfonyl chloride; N-methylimidazole / pyridine / 0.5 h
With
1-methyl-1H-imidazole; triisopropylbenzenesulfonyl chloride; tetrabutyl ammonium fluoride; dicyclohexyl-carbodiimide;
In
pyridine; diethyl ether; water; acetic acid;
1.1: Addition / 1.2: Condensation / 2.1: acidolysis / 3.1: Esterification / 4.1: Hydrolysis / 5.1: Esterification;
DOI:10.1007/BF02786343
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 75 percent / triisopropylbenzenesulfonyl chloride; M-methylimidazole / pyridine
2: 85 percent / tetrabutylammonium fluoride / pyridine; H2O / 5 h / 50 °C / pH 7.0
3: 70 percent / triisopropylbenzenesulfonyl chloride; N-methylimidazole / pyridine / 0.5 h
With
1-methyl-1H-imidazole; triisopropylbenzenesulfonyl chloride; tetrabutyl ammonium fluoride;
In
pyridine; water;
1: Esterification / 2: Hydrolysis / 3: Esterification;
DOI:10.1007/BF02786343
