(η5-C4Me2(Ph)HP)2TiCl2

Base Information

Chemical Name:(η5-C4Me2(Ph)HP)2TiCl2
CAS No.:516493-57-5
Molecular Formula:C₂₄H₂₄Cl₂P₂Ti
Molecular Weight:493.188
Hs Code.:

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Chemical Property of (η5-C4Me2(Ph)HP)2TiCl2

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Technology Process of (η5-C4Me2(Ph)HP)2TiCl2

There total 1 articles about (η5-C4Me2(Ph)HP)2TiCl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: titanium(IV) chloride tetrahydrofuran

: 515877-62-0
1-(trimethylstannyl)-3,4-dimethyl-2-phenylphosphole

: 516493-57-5,515877-60-8
(η5-C4Me2(Ph)HP)2TiCl2

Guidance literature:: In hexane; dichloromethane; soln. of stannylphosphole in C6H14 added rapidly to soln. of TiCl4*2THF in CH2Cl2 at room temp., mixt. stirred for 4 h; soln. concd., washed (C6H14), dried (vac.);
DOI:10.1039/b208945a

Reference yield: 35.0%

: 516493-57-5,515877-60-8
(η5-C4Me2(Ph)HP)2TiCl2

: 201230-82-2
carbon monoxide

: 516462-53-6,518307-11-4
bis(3,4-dimethyl-2-phenylphospholyl)titanium dicarbonyl

Guidance literature:: With Mg; In dichloromethane; pentane; to soln. Ti in THF Mg was added, CO was bubbled for 5 min and stirred overnight at 40°C; react. mixt. was concd., residue was extd. with pentane and concd.; elem. anal.;
DOI:10.1021/om020961h