4-methoxyphenyl 3-O-(6-methyl-3-O-benzyl-2,4-di-O-pivaloyl-α-L-idopyranuronosyl)-2-deoxy-4,6-O-(di-tert-butylsilylene)-2-trifluoroacetamido-β-D-galactopyranoside

Base Information

Chemical Name:4-methoxyphenyl 3-O-(6-methyl-3-O-benzyl-2,4-di-O-pivaloyl-α-L-idopyranuronosyl)-2-deoxy-4,6-O-(di-tert-butylsilylene)-2-trifluoroacetamido-β-D-galactopyranoside
CAS No.:1619227-51-8
Molecular Formula:C₄₇H₆₆F₃NO₁₅Si
Molecular Weight:970.119
Hs Code.:

4-methoxyphenyl 3-O-(6-methyl-3-O-benzyl-2,4-di-O-pivaloyl-α-L-idopyranuronosyl)-2-deoxy-4,6-O-(di-tert-butylsilylene)-2-trifluoroacetamido-β-D-galactopyranoside

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Chemical Property of 4-methoxyphenyl 3-O-(6-methyl-3-O-benzyl-2,4-di-O-pivaloyl-α-L-idopyranuronosyl)-2-deoxy-4,6-O-(di-tert-butylsilylene)-2-trifluoroacetamido-β-D-galactopyranoside

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Technology Process of 4-methoxyphenyl 3-O-(6-methyl-3-O-benzyl-2,4-di-O-pivaloyl-α-L-idopyranuronosyl)-2-deoxy-4,6-O-(di-tert-butylsilylene)-2-trifluoroacetamido-β-D-galactopyranoside

There total 2 articles about 4-methoxyphenyl 3-O-(6-methyl-3-O-benzyl-2,4-di-O-pivaloyl-α-L-idopyranuronosyl)-2-deoxy-4,6-O-(di-tert-butylsilylene)-2-trifluoroacetamido-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1619227-50-7
C₃₇H₅₀F₃NO₁₃Si

: 3282-30-2
pivaloyl chloride

: 1619227-51-8
4-methoxyphenyl 3-O-(6-methyl-3-O-benzyl-2,4-di-O-pivaloyl-α-L-idopyranuronosyl)-2-deoxy-4,6-O-(di-tert-butylsilylene)-2-trifluoroacetamido-β-D-galactopyranoside

Guidance literature:: With dmap; In pyridine; at 20 ℃; for 45h;
DOI:10.1002/ejoc.201402222

Reference yield:

: 1436409-71-0
4-methoxyphenyl 3-O-(methyl 3-O-benzyl-2,4-di-O-levulinoyl-α-L-idopyranosyluronate)-4,6-O-di-tert-butylsilylene-2-deoxy-2-trifluoroacetamido-β-D-galactopyranoside

: 1619227-51-8
4-methoxyphenyl 3-O-(6-methyl-3-O-benzyl-2,4-di-O-pivaloyl-α-L-idopyranuronosyl)-2-deoxy-4,6-O-(di-tert-butylsilylene)-2-trifluoroacetamido-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; hydrazine hydrate / dichloromethane; pyridine / 3 h / 20 °C

2: dmap / pyridine / 45 h / 20 °C

With dmap; hydrazine hydrate; acetic acid; In pyridine; dichloromethane;
DOI:10.1002/ejoc.201402222