indan-1,2,3-trione-2-(4-nitro-phenylhydrazone)

Base Information

• Chemical Name: indan-1,2,3-trione-2-(4-nitro-phenylhydrazone)
• CAS No.: 5103-49-1
• Molecular Formula: C₁₅H₉N₃O₄
• Molecular Weight: 295.254
• Mol file: 5103-49-1.mol

Synonyms:

Chemical Property of indan-1,2,3-trione-2-(4-nitro-phenylhydrazone)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of indan-1,2,3-trione-2-(4-nitro-phenylhydrazone)

There total 10 articles about indan-1,2,3-trione-2-(4-nitro-phenylhydrazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1H-indene-1,3(2H)-dione (606-23-5) + 4-nitrobenzenediazonium chloride (100-05-0) → indan-1,2,3-trione-2-(4-nitro-phenylhydrazone) (5103-49-1)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/ja01440a041

Reference yield:

1H-indene-1,3(2H)-dione (606-23-5) → indan-1,2,3-trione-2-(4-nitro-phenylhydrazone) (5103-49-1)

Guidance literature:

Multi-step reaction with 3 steps

1: Br₂, KOAc / acetic acid

2: ethanol

3: (i) (diazotization), (ii) /BRN= 2671477/, KOAc, EtOH

With bromine; potassium acetate; In ethanol; acetic acid;

Reference yield:

2-bromo-indan-1,3-dione (7319-63-3) → indan-1,2,3-trione-2-(4-nitro-phenylhydrazone) (5103-49-1)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol

2: (i) (diazotization), (ii) /BRN= 2671477/, KOAc, EtOH

In ethanol;

upstream raw materials:

1H-indene-1,3(2H)-dione

4-nitrobenzenediazonium chloride

p-nitrobenzenediazonium

1,3-dioxo-indan-2-carboxylic acid ethyl ester