(HC₆H₄CHC₆H₅Cr(CO)3)2NCH₃

Base Information

Chemical Name:(HC₆H₄CHC₆H₅Cr(CO)3)2NCH₃
CAS No.:67254-32-4
Molecular Formula:C₃₃H₂₅Cr₂NO₆
Molecular Weight:635.557
Hs Code.:

(HC<sub>6</sub>H<sub>4</sub>CHC<sub>6</sub>H<sub>5</sub>Cr(CO)3)2NCH<sub>3</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (HC₆H₄CHC₆H₅Cr(CO)3)2NCH₃

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Technology Process of (HC₆H₄CHC₆H₅Cr(CO)3)2NCH₃

There total 1 articles about (HC₆H₄CHC₆H₅Cr(CO)3)2NCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 12155-17-8
benzhydroltricarbonylchromium⁽⁰⁾

: 74-89-5
methylamine

: 67254-32-4,67235-59-0
(HC₆H₄CHC₆H₅Cr(CO)3)2NCH₃

Guidance literature:: With HPF₆*Et₂O; In dichloromethane; To a soln. of complex in CH2Cl2 was added HPF6*Et2O at -30°C with stirring (N2 atm.);, after 1 min CH3NH2 was added;; the mixt. was added to an ice-water, extd. with ether and CH2Cl2, the org. layer was dried over MgSO4, filtered, evapd., chromd. on silica gel ( benzene-hexane); elem. anal.;;
DOI:10.1016/S0022-328X(00)93566-6