Technology Process of C30H37NO5Se
There total 10 articles about C30H37NO5Se which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridinium p-toluenesulfonate / methanol / 20 °C
2: dmap; triethylamine / dichloromethane / 20 °C
3: lithium diisopropyl amide / tetrahydrofuran / -78 °C
4: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C
5: lithium diisopropyl amide / tetrahydrofuran / -78 °C
With
dmap; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.05.065
- Guidance literature:
-
Multi-step reaction with 9 steps
1: ethanol; sodium / tetrahydrofuran / 20 °C
2: sodium chloride / dimethyl sulfoxide / 150 °C
3: trimethylaluminum; ammonium chloride / toluene / 40 °C
4: sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / 150 °C
5: pyridinium p-toluenesulfonate / methanol / 20 °C
6: dmap; triethylamine / dichloromethane / 20 °C
7: lithium diisopropyl amide / tetrahydrofuran / -78 °C
8: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C
9: lithium diisopropyl amide / tetrahydrofuran / -78 °C
With
dmap; ethanol; trimethylaluminum; sodium; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; ammonium chloride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; sodium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1016/j.bmcl.2012.05.065