Technology Process of 4-(tert-butyldiphenylsiloxy)butyl methyl adipate
There total 6 articles about 4-(tert-butyldiphenylsiloxy)butyl methyl adipate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 75 percent / methanol / 2 h / Ambient temperature
2: 46 percent / CrO3, H2SO4 / acetone; H2O / 0.67 h / Ambient temperature
3: oxalyl chloride, DMF / CH2Cl2 / 17 h / Ambient temperature
4: 1) NaH, imidazole / 1) THF, mineral oil, room temp., 19 h, 2) THF, reflux, 4 h
With
1H-imidazole; chromium(VI) oxide; oxalyl dichloride; sulfuric acid; sodium hydride; N,N-dimethyl-formamide;
In
methanol; dichloromethane; water; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 46 percent / CrO3, H2SO4 / acetone; H2O / 0.67 h / Ambient temperature
2: oxalyl chloride, DMF / CH2Cl2 / 17 h / Ambient temperature
3: 1) NaH, imidazole / 1) THF, mineral oil, room temp., 19 h, 2) THF, reflux, 4 h
With
1H-imidazole; chromium(VI) oxide; oxalyl dichloride; sulfuric acid; sodium hydride; N,N-dimethyl-formamide;
In
dichloromethane; water; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: oxalyl chloride, DMF / CH2Cl2 / 17 h / Ambient temperature
2: 1) NaH, imidazole / 1) THF, mineral oil, room temp., 19 h, 2) THF, reflux, 4 h
With
1H-imidazole; oxalyl dichloride; sodium hydride; N,N-dimethyl-formamide;
In
dichloromethane;
