4-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-3-(7-chloro-6-fluorobenzo[d]thiazol-2-ylamino)-4,5-dihydro-1H-pyrazol-5-yl)-2-methoxyphenol

Base Information

Chemical Name:4-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-3-(7-chloro-6-fluorobenzo[d]thiazol-2-ylamino)-4,5-dihydro-1H-pyrazol-5-yl)-2-methoxyphenol
CAS No.:1311166-21-8
Molecular Formula:C₂₄H₁₅Cl₂F₂N₅O₂S₂
Molecular Weight:578.45
Hs Code.:

4-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-3-(7-chloro-6-fluorobenzo[d]thiazol-2-ylamino)-4,5-dihydro-1H-pyrazol-5-yl)-2-methoxyphenol

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Chemical Property of 4-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-3-(7-chloro-6-fluorobenzo[d]thiazol-2-ylamino)-4,5-dihydro-1H-pyrazol-5-yl)-2-methoxyphenol

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Technology Process of 4-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-3-(7-chloro-6-fluorobenzo[d]thiazol-2-ylamino)-4,5-dihydro-1H-pyrazol-5-yl)-2-methoxyphenol

There total 4 articles about 4-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-3-(7-chloro-6-fluorobenzo[d]thiazol-2-ylamino)-4,5-dihydro-1H-pyrazol-5-yl)-2-methoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 218155-19-2
7-chloro-6-fluoro-2-hydrazinylbenzo[d]thiazole

: 1311166-15-0
N-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-3-(4-hydroxy-3-methoxyphenyl)acrylamide

: 1311166-21-8
4-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-3-(7-chloro-6-fluorobenzo[d]thiazol-2-ylamino)-4,5-dihydro-1H-pyrazol-5-yl)-2-methoxyphenol

Guidance literature:: With acetic acid; In ethanol; for 8h; Reflux;
DOI:10.1002/ardp.201100072

Reference yield:

: 101337-93-3
2-amino-6-fluoro-7-chloro-1,3-benzothiazole

: 1311166-21-8
4-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-3-(7-chloro-6-fluorobenzo[d]thiazol-2-ylamino)-4,5-dihydro-1H-pyrazol-5-yl)-2-methoxyphenol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; hydrazine hydrate / water; ethylene glycol / 2 h / 5 - 10 °C / Reflux

2: acetic acid / ethanol / 8 h / Reflux

With hydrogenchloride; hydrazine hydrate; acetic acid; In ethanol; water; ethylene glycol;
DOI:10.1002/ardp.201100072

Reference yield:

: 367-21-5
3-chloro-4-fluorophenylamine

: 1311166-21-8
4-(1-(7-chloro-6-fluorobenzo[d]thiazol-2-yl)-3-(7-chloro-6-fluorobenzo[d]thiazol-2-ylamino)-4,5-dihydro-1H-pyrazol-5-yl)-2-methoxyphenol

Guidance literature:: Multi-step reaction with 3 steps

1: bromine; acetic acid / 14 h / 5 - 20 °C

2: hydrogenchloride; hydrazine hydrate / water; ethylene glycol / 2 h / 5 - 10 °C / Reflux

3: acetic acid / ethanol / 8 h / Reflux

With hydrogenchloride; bromine; hydrazine hydrate; acetic acid; In ethanol; water; ethylene glycol;
DOI:10.1002/ardp.201100072