C₁₇H₁₉N₃O₆

Base Information

• Chemical Name: C₁₇H₁₉N₃O₆
• CAS No.: 1422023-29-7
• Molecular Formula: C₁₇H₁₉N₃O₆
• Molecular Weight: 361.354
• Mol file: 1422023-29-7.mol

Synonyms:

Chemical Property of C₁₇H₁₉N₃O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₉N₃O₆

There total 4 articles about C₁₇H₁₉N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

vegfrecine (1422273-23-1) + chloromethyl methyl ether (107-30-2) → C17H19N3O6 (1422023-29-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1021/np300535c

Reference yield:

C31H43N3O5Si2 (1422023-30-0) → C17H19N3O6 (1422023-29-7)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonia / methanol / 2 h / 20 °C

2: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With tetrabutyl ammonium fluoride; ammonia; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1021/np300535c

Reference yield:

2-amino-phenol (95-55-6) → C17H19N3O6 (1422023-29-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2: sodium periodate / methanol; water / 20 °C

3: ammonia / methanol / 2 h / 20 °C

4: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 20 °C

5: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With 1H-imidazole; sodium periodate; tetrabutyl ammonium fluoride; ammonia; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

DOI:10.1021/np300535c

upstream raw materials:

vegfrecine

chloromethyl methyl ether

2-amino-phenol

O-tert-butyldimethylsilyl-2-aminophenol