Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

Base Information

• Chemical Name: Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine
• CAS No.: 98815-92-0
• Molecular Formula: C₆H₁₅N*C₅₁H₅₇N₆O₁₁PSi
• Molecular Weight: 1090.3

Synonyms:

Chemical Property of Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

There total 4 articles about Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Nitro-benzaldehyde oxime; compound with triethyl-amine + Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2,5-dichloro-phenyl ester 2-(4-nitro-phenyl)-ethyl ester (98815-89-5) → Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine (98815-92-0)

Guidance literature:

In 1,4-dioxane; water; at 20 ℃; for 0.833333h;

DOI:10.1016/S0040-4039(00)94778-6

Reference yield:

N-[9-((R)-2-Hydroxy-1-{(S)-1-hydroxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl)-9H-purin-6-yl]-benzamide (98815-82-8) → Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine (98815-92-0)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine

3: H₂O; dioxane / 0.83 h / 20 °C

In 1,4-dioxane; pyridine; water;

DOI:10.1016/S0040-4039(00)94778-6

Reference yield:

N-[9-((R)-2-(tert-Butyl-dimethyl-silanyloxy)-1-{(S)-1-hydroxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl)-9H-purin-6-yl]-benzamide (98815-84-0) → Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine (98815-92-0)

Guidance literature:

Multi-step reaction with 2 steps

2: H₂O; dioxane / 0.83 h / 20 °C

In 1,4-dioxane; water;

DOI:10.1016/S0040-4039(00)94778-6

upstream raw materials:

Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2,5-dichloro-phenyl ester 2-(4-nitro-phenyl)-ethyl ester

N-[9-((R)-2-Hydroxy-1-{(S)-1-hydroxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl)-9H-purin-6-yl]-benzamide

N-[9-((R)-2-(tert-Butyl-dimethyl-silanyloxy)-1-{(S)-1-hydroxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl)-9H-purin-6-yl]-benzamide

tert-butyldimethylsilyl chloride

Downstream raw materials:

C₈₂H₈₂N₁₁O₁₇PSi

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