Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2,5-dichloro-phenyl ester 2-(4-nitro-phenyl)-ethyl ester

Base Information

• Chemical Name: Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2,5-dichloro-phenyl ester 2-(4-nitro-phenyl)-ethyl ester
• CAS No.: 98815-89-5
• Molecular Formula: C₅₇H₅₉Cl₂N₆O₁₁PSi
• Molecular Weight: 1134.09

Synonyms:

Chemical Property of Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2,5-dichloro-phenyl ester 2-(4-nitro-phenyl)-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2,5-dichloro-phenyl ester 2-(4-nitro-phenyl)-ethyl ester

There total 2 articles about Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2,5-dichloro-phenyl ester 2-(4-nitro-phenyl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[9-((R)-2-Hydroxy-1-{(S)-1-hydroxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl)-9H-purin-6-yl]-benzamide (98815-82-8) → Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2,5-dichloro-phenyl ester 2-(4-nitro-phenyl)-ethyl ester (98815-89-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

In pyridine;

DOI:10.1016/S0040-4039(00)94778-6

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) → Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2,5-dichloro-phenyl ester 2-(4-nitro-phenyl)-ethyl ester (98815-89-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

In pyridine;

DOI:10.1016/S0040-4039(00)94778-6

Reference yield:

4-Nitro-benzaldehyde oxime; compound with triethyl-amine + Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2,5-dichloro-phenyl ester 2-(4-nitro-phenyl)-ethyl ester (98815-89-5) → Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine (98815-92-0)

Guidance literature:

In 1,4-dioxane; water; at 20 ℃; for 0.833333h;

DOI:10.1016/S0040-4039(00)94778-6

upstream raw materials:

N-[9-((R)-2-Hydroxy-1-{(S)-1-hydroxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl)-9H-purin-6-yl]-benzamide

tert-butyldimethylsilyl chloride

Downstream raw materials:

Phosphoric acid (R)-2-[(R)-1-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-propyl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

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