C₂₄H₃₃N₅O₃

Base Information

Chemical Name:C₂₄H₃₃N₅O₃
CAS No.:1062671-14-0
Molecular Formula:C₂₄H₃₃N₅O₃
Molecular Weight:439.558
Hs Code.:

C<sub>24</sub>H<sub>33</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:

Suppliers and Price of C₂₄H₃₃N₅O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₄H₃₃N₅O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₄H₃₃N₅O₃

There total 13 articles about C₂₄H₃₃N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₀N₄O₃

: 1062671-14-0
C₂₄H₃₃N₅O₃

Guidance literature:: With ammonia; In methanol; at 60 ℃; Sealed tube; Inert atmosphere;
DOI:10.1021/jm4014696

Reference yield:

: 75308-46-2
tert-butyl 2,6-dichloropyridine-4-carboxylate

: 1062671-14-0
C₂₄H₃₃N₅O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: 72 h / 100 °C / Sealed tube; Inert atmosphere

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; tetrahydrofuran / 16 h / 75 °C / Inert atmosphere

3.1: hydrogenchloride / water / 24 h / 80 °C

4.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia / 1,4-dioxane; N,N-dimethyl-formamide / 2.25 h / 0 °C / Inert atmosphere

4.2: 17 h / 20 - 70 °C / Inert atmosphere

5.1: hydroxylamine hydrochloride; potassium tert-butylate / methanol / 15 h / 60 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 20 °C / Inert atmosphere

6.2: 80 - 100 °C / Inert atmosphere

7.1: sodium hydroxide / water; isopropyl alcohol / 20 °C

8.1: ammonia / methanol / 60 °C / Sealed tube; Inert atmosphere

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; hydroxylamine hydrochloride; potassium tert-butylate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm4014696

Reference yield:

: 1365337-45-6
tert-butyl 2-(diethylamino)-6-methylisonicotinate

: 1062671-14-0
C₂₄H₃₃N₅O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / water / 24 h / 80 °C

2.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia / 1,4-dioxane; N,N-dimethyl-formamide / 2.25 h / 0 °C / Inert atmosphere

2.2: 17 h / 20 - 70 °C / Inert atmosphere

3.1: hydroxylamine hydrochloride; potassium tert-butylate / methanol / 15 h / 60 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 20 °C / Inert atmosphere

4.2: 80 - 100 °C / Inert atmosphere

5.1: sodium hydroxide / water; isopropyl alcohol / 20 °C

6.1: ammonia / methanol / 60 °C / Sealed tube; Inert atmosphere

With hydrogenchloride; hydroxylamine hydrochloride; potassium tert-butylate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm4014696