cis-P,P'-([5,11,17,23-tetra-tert-butyl-25,27-dipropoxy-26,28-bis(diphenoxyphosphanyloxy)calix[4]arene]-1,5-cyclooctadiene)rhodium(I) tetrafluoroborate

Base Information

Chemical Name:cis-P,P'-([5,11,17,23-tetra-tert-butyl-25,27-dipropoxy-26,28-bis(diphenoxyphosphanyloxy)calix[4]arene]-1,5-cyclooctadiene)rhodium(I) tetrafluoroborate
CAS No.:851769-80-7
Molecular Formula:BF₄*C₈₂H₉₈O₈P₂Rh
Molecular Weight:1463.33
Hs Code.:

cis-P,P'-([5,11,17,23-tetra-tert-butyl-25,27-dipropoxy-26,28-bis(diphenoxyphosphanyloxy)calix[4]arene]-1,5-cyclooctadiene)rhodium(I) tetrafluoroborate

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Chemical Property of cis-P,P'-([5,11,17,23-tetra-tert-butyl-25,27-dipropoxy-26,28-bis(diphenoxyphosphanyloxy)calix[4]arene]-1,5-cyclooctadiene)rhodium(I) tetrafluoroborate

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Technology Process of cis-P,P'-([5,11,17,23-tetra-tert-butyl-25,27-dipropoxy-26,28-bis(diphenoxyphosphanyloxy)calix[4]arene]-1,5-cyclooctadiene)rhodium(I) tetrafluoroborate

There total 1 articles about cis-P,P'-([5,11,17,23-tetra-tert-butyl-25,27-dipropoxy-26,28-bis(diphenoxyphosphanyloxy)calix[4]arene]-1,5-cyclooctadiene)rhodium(I) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 851769-90-9
5,11,17,23-tetra-tert-butyl-25,27-dipropoxy-26,28-bis(diphenoxyphosphanyloxy)calix[4]arene

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 14104-20-2
silver tetrafluoroborate

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: 851769-80-7
cis-P,P'-([5,11,17,23-tetra-tert-butyl-25,27-dipropoxy-26,28-bis(diphenoxyphosphanyloxy)calix[4]arene]-1,5-cyclooctadiene)rhodium(I) tetrafluoroborate

Guidance literature:: In tetrahydrofuran; dichloromethane; byproducts: AgCl; (N2); addn. of a soln. of silver salt in THF to a soln. of rhodium complex in CH2Cl2, stirring for 5 min, decantation, filtration through Celite, addn. to a soln. of ligand in CH2Cl2, react. for 1 h; concn., addn. of hexane; elem. anal.;
DOI:10.1039/b419284b