[(CH₃)2NCH₂]B₅H₈

Base Information

• Chemical Name: [(CH₃)2NCH₂]B₅H₈
• CAS No.: 99657-83-7
• Molecular Formula: C₃H₁₆B₅N
• Molecular Weight: 120.222
• Mol file: 99657-83-7.mol

Synonyms:

Chemical Property of [(CH₃)2NCH₂]B₅H₈

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of [(CH₃)2NCH₂]B₅H₈

There total 1 articles about [(CH₃)2NCH₂]B₅H₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.3%

Li(1+)*B5H8(1-)=LiB5H8 (34370-18-8) + eschenmoser's salt (33797-51-2) → [(CH3)2NCH2]B5H8 (99657-83-7) + trimethylamine borane (1231953-83-5) + lithium iodide (10377-51-2)

Guidance literature:

In diethyl ether; React. of starting compd. under N2 at -78°C with stirring, slow warming after 1 h to -10°C over a period of 2 h.; Distg. of volatile materials into -63 (white solid) and -196°C (ether, B5H9) U-traps. Further purifn. of solid by fractional condensation (-45°C). Distn. of B5H8-compd. requires several days, because of its low volatility. Elem. anal.;

upstream raw materials:

Li⁽¹⁺⁾*B₅H₈^(1-)=LiB₅H₈

eschenmoser's salt