tert-butyl 1-methylcyclohexanecarboperoxoate

Base Information

• Chemical Name: tert-butyl 1-methylcyclohexanecarboperoxoate
• CAS No.: 25023-15-8
• Molecular Formula: C₁₂H₂₂O₃
• Molecular Weight: 214.305
• Mol file: 25023-15-8.mol

Synonyms:

Chemical Property of tert-butyl 1-methylcyclohexanecarboperoxoate

Chemical Property:

• Vapor Pressure: 0.0198mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyl 1-methylcyclohexanecarboperoxoate

There total 3 articles about tert-butyl 1-methylcyclohexanecarboperoxoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-1-cyclohexanecarboxylic acid (1123-25-7) → 1-Methyl-cyclohexan-percarbonsaeure-tert.-butylester (25023-15-8)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂

2: Py / CH₂Cl₂

With pyridine; thionyl chloride; In dichloromethane;

Reference yield:

1-Methylcyclohexanol (590-67-0) → 1-Methyl-cyclohexan-percarbonsaeure-tert.-butylester (25023-15-8)

Guidance literature:

Multi-step reaction with 3 steps

2: SOCl₂

3: Py / CH₂Cl₂

With pyridine; thionyl chloride; In dichloromethane;

Reference yield:

tert.-butylhydroperoxide (75-91-2) + 1-methyl-1-cyclohexancarboxylic acid chloride (2890-61-1) → 1-Methyl-cyclohexan-percarbonsaeure-tert.-butylester (25023-15-8)

Guidance literature:

With pyridine; In dichloromethane;

upstream raw materials:

tert.-butylhydroperoxide

1-methyl-1-cyclohexancarboxylic acid chloride

1-methyl-1-cyclohexanecarboxylic acid

1-Methylcyclohexanol