Technology Process of 1-piperidin
There total 10 articles about 1-piperidin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
for 16h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 67 percent / LiAlH4 / diethyl ether / 1 h / Ambient temperature
2: 53 percent / VO(acac)2, tert-butylhydroperoxide / benzene / 48 h / 40 °C
3: 92 percent / CrO3, pyridine / CH2Cl2 / 0.25 h / Ambient temperature
4: 60 percent / hydrazine hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature
5: 85 percent / Hg(II)-acetate / 1) 75 deg , 2 h; 2) 1 h, reflux
6: 58 percent / 1 h / 200 °C
7: 94 percent / H2 / Pt-oxide / acetic acid / 1 h
8: 62 percent / K2CO3 / 16 h / Ambient temperature
With
pyridine; chromium(VI) oxide; tert.-butylhydroperoxide; lithium aluminium tetrahydride; bis(acetylacetonate)oxovanadium; mercury(II) diacetate; hydrogen; potassium carbonate; hydrazine hydrate; acetic acid;
Pt-oxide;
In
diethyl ether; ethanol; dichloromethane; acetic acid; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 60 percent / hydrazine hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature
2: 85 percent / Hg(II)-acetate / 1) 75 deg , 2 h; 2) 1 h, reflux
3: 58 percent / 1 h / 200 °C
4: 94 percent / H2 / Pt-oxide / acetic acid / 1 h
5: 62 percent / K2CO3 / 16 h / Ambient temperature
With
mercury(II) diacetate; hydrogen; potassium carbonate; hydrazine hydrate; acetic acid;
Pt-oxide;
In
ethanol; acetic acid;
