methyldiphenylphosphonium cyclopentadienylide

Base Information

Chemical Name:methyldiphenylphosphonium cyclopentadienylide
CAS No.:58109-59-4
Molecular Formula:C₁₈H₁₇P
Molecular Weight:264.307
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyldiphenylphosphonium cyclopentadienylide

Chemical Property:

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Technology Process of methyldiphenylphosphonium cyclopentadienylide

There total 2 articles about methyldiphenylphosphonium cyclopentadienylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: cyclopentadienylthallium(I)

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 74-88-4
methyl iodide

: 58109-59-4
methyldiphenylphosphonium cyclopentadienylide

Guidance literature:: cyclopentadienylthallium(I); chloro-diphenylphosphine; In diethyl ether;

methyl iodide; In diethyl ether;

With lithium hexamethyldisilazane; In tetrahydrofuran; at -70 - 20 ℃;

Reference yield:

: 58109-59-4
methyldiphenylphosphonium cyclopentadienylide

Guidance literature:: entspr. J-Dimeren <11> u. BuLi;
DOI:10.1016/0040-4020(75)80333-4

Reference yield: 61.0%

: 58109-59-4
methyldiphenylphosphonium cyclopentadienylide

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 934000-50-7
[(η5-methyldiphenylphosphonium cyclopentadienylide)Cr(CO)3]

Guidance literature:: In diethylene glycol dimethyl ether; (Ar); refluxing soln. of chromium compd. and phosphorus compd. in diglyme for 3 h; cooling, filtration, washing solid with diglyme, addn. of hexane to filtrate, collecting precipitate, washing with hexane, drying in vac., elem.anal.;
DOI:10.1021/om070018j