bis(dimethylamido)[bis(tert-butylamido)phenylborane]titanium(IV)

Base Information

Chemical Name:bis(dimethylamido)[bis(tert-butylamido)phenylborane]titanium(IV)
CAS No.:562809-57-8
Molecular Formula:C₁₈H₃₅BN₄Ti
Molecular Weight:366.194
Hs Code.:

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Chemical Property of bis(dimethylamido)[bis(tert-butylamido)phenylborane]titanium(IV)

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Technology Process of bis(dimethylamido)[bis(tert-butylamido)phenylborane]titanium(IV)

There total 1 articles about bis(dimethylamido)[bis(tert-butylamido)phenylborane]titanium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.4%

: 16753-20-1
bis(dimethylamido)titanium(IV) dichloride

: 124652-56-8
bis(tert-butylamino)phenylborane dilithium salt

: 562809-57-8
bis(dimethylamido)[bis(tert-butylamido)phenylborane]titanium(IV)

Guidance literature:: In pentane; byproducts: LiCl; under N2; pentane solns. of Ti compd. and B compd. frozen upon dissolution; upon thawing B compd. soln. added dropwise (over 7 min) to partiallythawed Ti compd. soln.; warmed slowly to room temp.; stirred overnight; filtered through Celite; solvent removed from filtrate by vac. evapn.; liq. refiltered through fresh Celite; filtrate evapd. under vac. for 12 h; solid collected; elem. anal.;
DOI:10.1016/S0020-1693(02)01352-X

Reference yield: 90.5%

: 75-77-4
chloro-trimethyl-silane

: 562809-57-8
bis(dimethylamido)[bis(tert-butylamido)phenylborane]titanium(IV)

: dichloro[bis(tert-butylamido)phenylborane]titanium(IV)

Guidance literature:: In further solvent(s); under N2; hexane-Me3SiCl soln. of Ti complex stirred overnight; ppt. collected by filtration; filtrate concd.; additional ppt. collected; combined solid washed with cold hexanes; elem. anal.;
DOI:10.1016/S0020-1693(02)01352-X