2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-ONE OXIME

Base Information

• Chemical Name: 2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-ONE OXIME
• CAS No.: 23240-52-0
• Molecular Formula: C₁₂H₁₂N₂O
• Molecular Weight: 200.24
• Mol file: 23240-52-0.mol

Synonyms:

Chemical Property of 2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-ONE OXIME

Chemical Property:

Purity/Quality:

2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-ONE OXIME 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-ONE OXIME

There total 2 articles about 2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-ONE OXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1-oxo-2,3,4,9-tetrahydrocarbazole (3456-99-3) → 1-Hydroxyimino-1,2,3,4-tetrahydrocarbazole (23240-52-0)

Guidance literature:

With pyridine; hydroxylamine hydrochloride; In ethanol; for 1h; Heating;

Reference yield:

1-oxo-2,3,4,9-tetrahydrocarbazole (3456-99-3) → (Z)-2,3,4,9-tetrahydro-1H-carbazol-1-one oxime (23240-49-5) + 1-Hydroxyimino-1,2,3,4-tetrahydrocarbazole (23240-52-0)

Guidance literature:

With pyridine; hydroxylamine hydrochloride; at 20 ℃;

DOI:10.1021/jo902177p

upstream raw materials:

1-oxo-2,3,4,9-tetrahydrocarbazole

Refernces

• 1、 -. "NOVEL CYCLOALKYL’B! CONDENSED INDOLES". Page 38. . Retrieved 2008/06/13.