methyl Hexadecanoate

Base Information

Chemical Name:methyl Hexadecanoate
CAS No.:130277-55-3
Molecular Formula:C₂₃H₄₄O₆
Molecular Weight:416.599
Hs Code.:

<DL-(1,2,3,5/4)-2,3,4,5-Tetrahydroxycyclohexyl>methyl Hexadecanoate

Synonyms:

Suppliers and Price of methyl Hexadecanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl Hexadecanoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of methyl Hexadecanoate

There total 27 articles about methyl Hexadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 130277-54-2,130324-59-3
methyl Hexadecanoate

: 112314-16-6,130324-60-6,130324-66-2,141436-56-8,141436-57-9,141436-62-6,141436-63-7
DL-(1,3,5/2,4)-5-Methylcyclohexane-1,2,3,4-tetrol

: 112314-16-6,130324-60-6,130324-66-2,141436-56-8,141436-57-9,141436-62-6,141436-63-7
DL-(1,3/2,4,5)-5-Methylcyclohexane-1,2,3,4-tetrol

: 130277-55-3,130324-82-2
methyl Hexadecanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 25 ℃; for 4h; under 760 Torr; Yield given;
DOI:10.1002/hlca.19900730428

Reference yield: 4.0%

: 130277-54-2,130324-59-3
methyl Hexadecanoate

: 130277-57-5
(1,3,5/2)-5-Methylcyclohexane-1,2,3-triol

: 130277-56-4
methyl Hexadecanoate

: 130277-55-3,130324-82-2
methyl Hexadecanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 25 ℃; for 2h; under 760 Torr; Further byproducts given;
DOI:10.1002/hlca.19900730428

Reference yield:

: 87-89-8
D-myo-inositol

: 130277-55-3,130324-82-2
methyl Hexadecanoate

Guidance literature:: Multi-step reaction with 12 steps

1: 93 percent / TsOH / toluene; dimethylformamide / 9 h / Heating

2: 183 g / KOH / 0.5 h / 120 °C

3: 85 percent / AcOH / H₂O / 1.5 h / 80 - 100 °C

4: 1.) Bu₂SnO / 1.) toluene, 110 deg C; 2.) DMF, 80 deg C

5: NaH / dimethylformamide / 4 h / 40 °C

6: TsOH / 5percent Pd/C / aq. ethanol / 22 h / Heating

7: 72 percent / pyridinium chlorochromate / CH₂Cl₂ / 24 h / 25 °C

8: 25 percent / BuLi / tetrahydrofuran / 0.75 h / 0 - 21 °C

9: 24 percent / BF₃*Et₂O / diethyl ether / 1.5 h / Heating

10: 92 percent / NaBH₄ / ethanol / 0.42 h / Ambient temperature

11: 100 percent / pyridine / DMAP / CH₂Cl₂ / 2 h / Ambient temperature

12: 25 percent / hydrogen / 5percent Pd/C / ethanol / 4 h / 25 °C / 760 Torr

With pyridine; potassium hydroxide; sodium tetrahydroborate; n-butyllithium; boron trifluoride diethyl etherate; hydrogen; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; acetic acid; pyridinium chlorochromate; dmap; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/hlca.19900730428