Technology Process of Benzene, (2-cyclohexyl-1-propenyl)-, (E)-
There total 8 articles about Benzene, (2-cyclohexyl-1-propenyl)-, (E)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1-cyclohexyl-2,4,6-triphenylpyridin-1-ium tetrafluoroborate salt;
With
nickel(II) bromide dimethoxyethane; potassium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine;
at 20 ℃;
Schlenk technique;
Sealed tube;
Inert atmosphere;
1-Phenylprop-1-yne;
With
1,1,3,3-Tetramethyldisiloxane;
In
N,N-dimethyl acetamide;
at 20 ℃;
regioselective reaction;
Schlenk technique;
Sealed tube;
Inert atmosphere;
DOI:10.1039/c9cc05385a
- Guidance literature:
-
1-Phenylprop-1-yne; Cyclohexyl iodide;
With
nickel(II) bromide dimethoxyethane; potassium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine;
In
N,N-dimethyl acetamide;
for 0.0833333h;
Schlenk technique;
Inert atmosphere;
With
diethoxymethylsilane;
In
N,N-dimethyl acetamide;
at 30 ℃;
for 10h;
Reagent/catalyst;
Solvent;
stereoselective reaction;
Schlenk technique;
Inert atmosphere;
DOI:10.1039/c8cc01577e
- Guidance literature:
-
With
1,1,3,3-Tetramethyldisiloxane; nickel(II) chloride2-methoxyethyl ether; calcium acetate; 4,4'-di-tert-butyl-2,2'-bipyridine;
In
N,N-dimethyl acetamide;
at 40 ℃;
for 4h;
regioselective reaction;
Schlenk technique;
Inert atmosphere;
DOI:10.1016/j.tet.2018.10.037