chlorotris(2-(diphenylphosphino)ethyl)amineplatinum(II) chloride

Base Information

Chemical Name:chlorotris(2-(diphenylphosphino)ethyl)amineplatinum(II) chloride
CAS No.:855995-23-2
Molecular Formula:C₄₂H₄₂ClNP₃Pt*Cl
Molecular Weight:919.709
Hs Code.:

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Chemical Property of chlorotris(2-(diphenylphosphino)ethyl)amineplatinum(II) chloride

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Technology Process of chlorotris(2-(diphenylphosphino)ethyl)amineplatinum(II) chloride

There total 1 articles about chlorotris(2-(diphenylphosphino)ethyl)amineplatinum(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 15114-55-3
tris(2-(diphenylphosphino)ethyl)amine

: 855995-23-2,137355-03-4,114075-08-0
chlorotris(2-(diphenylphosphino)ethyl)amineplatinum(II) chloride

Guidance literature:: In acetone; refluxing (4-5 h); cooling,; ppt. filtered, washed with acetone; recrystd. from ethanol/Et2O; elem. anal.;

Reference yield: 41.0%

: 16940-66-2
sodium tetrahydroborate

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 114075-08-0,137355-03-4,1446323-87-0,855995-23-2
{PtCl(N(CH₂CH₂P(C₆H₅)2)3)}⁽¹⁺⁾*Cl^(1-)={PtCl(N(CH₂CH₂P(C₆H₅)2)3)}Cl

: 143-66-8
sodium tetraphenyl borate

: {Pt(AuP(C₆H₅)3)(N(CH₂CH₂P(C₆H₅)2)3)}⁽¹⁺⁾*{B(C₆H₅)4}^(1-)={Pt(AuP(C₆H₅)3)(N(CH₂CH₂P(C₆H₅)2)3)}{B(C₆H₅)4}

Guidance literature:: In methanol; dichloromethane; an equimol. mixt. of the Pt-chlorocomplex and NaBH4 was stirred for 30 min, evapd. to dryness in vac. and redissolved in THF; and stirred with AuCl(PPh3) for 30 min; the prod. was pptd. by addn. of NaBPh4;; the prod. was filtered off, washed twice with water and twice with methanol, and recrystd. from CH2Cl2/MeOH; elem.anal.;;
DOI:10.1039/DT9910002459