Ethanamine, 2-(diphenylphosphino)-N,N-bis[2-(diphenylphosphino)ethyl]-

Base Information

Chemical Name:Ethanamine, 2-(diphenylphosphino)-N,N-bis[2-(diphenylphosphino)ethyl]-
CAS No.:15114-55-3
Molecular Formula:C42H42NP3
Molecular Weight:653.723
Hs Code.:

Synonyms:

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Chemical Property of Ethanamine, 2-(diphenylphosphino)-N,N-bis[2-(diphenylphosphino)ethyl]-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Ethanamine, 2-(diphenylphosphino)-N,N-bis[2-(diphenylphosphino)ethyl]-

There total 2 articles about Ethanamine, 2-(diphenylphosphino)-N,N-bis[2-(diphenylphosphino)ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 817-09-4
tris-(2-chloroethyl)amine hydrochloride

: 829-85-6
diphenylphosphane

: 15114-55-3
tris(2-(diphenylphosphino)ethyl)amine

Guidance literature:: diphenylphosphane; With potassium tert-butylate; In tetrahydrofuran; for 0.25h;

tris-(2-chloroethyl)amine hydrochloride; In tetrahydrofuran; at 80 ℃; for 20h; Further stages.;
DOI:10.1039/b106021j

Reference yield:

: 15114-55-3
tris(2-(diphenylphosphino)ethyl)amine

Guidance literature:: Tris-(2-chlor-ethyl)-amin, K-diphenylphosphid-2-dioxan;
DOI:10.1021/ja01022a020

Reference yield: 95.0%

: 15114-55-3
tris(2-(diphenylphosphino)ethyl)amine

: silver nitrate

: 439119-78-5,152015-05-9
(Ag(tris(2-(diphenylphosphino)ethyl)amine)) nitrate

Guidance literature:: In dichloromethane; acetonitrile; addn. of ligand to a stirred soln. of AgNO3 in CH3CN/CH2Cl2 under N2 or Ar, stirring at room temp. for 2 h; addn. of Et2O, pptn., recrystn. from CH3CN/Et2O;