sodium 2-[(4-triflouromethyl-benzoyl)-hydrazono]-propionate

Base Information

• Chemical Name: sodium 2-[(4-triflouromethyl-benzoyl)-hydrazono]-propionate
• CAS No.: 1391436-65-9
• Molecular Formula: C₁₁H₈F₃N₂O₃*Na
• Molecular Weight: 296.181
• Mol file: 1391436-65-9.mol

Synonyms:

Chemical Property of sodium 2-[(4-triflouromethyl-benzoyl)-hydrazono]-propionate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of sodium 2-[(4-triflouromethyl-benzoyl)-hydrazono]-propionate

There total 1 articles about sodium 2-[(4-triflouromethyl-benzoyl)-hydrazono]-propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

4-(trifluoromethyl)benzoic acid hydrazide (339-59-3) + sodium pyruvate (113-24-6) → sodium 2-[(4-triflouromethyl-benzoyl)-hydrazono]-propionate (1391436-65-9)

Guidance literature:

In methanol; water; for 2h; Reflux;

DOI:10.1039/c2dt30322a

Reference yield: 36.0%

copper(II) choride dihydrate + sodium 2-[(4-triflouromethyl-benzoyl)-hydrazono]-propionate (1391436-65-9) → [Cu(2-[(4-trifluoromethylbenzoyl)-hydrazono]-propionate(2-))(H2O)2]*0.27H2O

Guidance literature:

In methanol; to soln. pyruvate-based aroyl-hydrazone in MeOH CuCl2*2H2O was added, stirred for 2 h; soln. was evapd. slowly, residue was washed with water, dissolved in MeOH and allowed to evaporate slowly at room temp., product was dried in vacuo; elem. anal.;

DOI:10.1039/c2dt30322a

Reference yield:

sodium 2-[(4-triflouromethyl-benzoyl)-hydrazono]-propionate (1391436-65-9) → 4-(trifluoromethyl)benzoic acid hydrazide (339-59-3)

Guidance literature:

With water; In dimethyl sulfoxide; at 37 ℃; pH=7.4; aq. phosphate buffer;

DOI:10.1039/c2dt30322a

upstream raw materials:

4-(trifluoromethyl)benzoic acid hydrazide

sodium pyruvate

Downstream raw materials:

4-(trifluoromethyl)benzoic acid hydrazide

Refernces