C₄₀H₆₆BrNO₁₂Si

Base Information

Chemical Name:C₄₀H₆₆BrNO₁₂Si
CAS No.:1448441-40-4
Molecular Formula:C₄₀H₆₆BrNO₁₂Si
Molecular Weight:860.953
Hs Code.:

C<sub>40</sub>H<sub>66</sub>BrNO<sub>12</sub>Si

Synonyms:

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Chemical Property of C₄₀H₆₆BrNO₁₂Si

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Technology Process of C₄₀H₆₆BrNO₁₂Si

There total 10 articles about C₄₀H₆₆BrNO₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₆₁BrO₁₂Si

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1448441-40-4
C₄₀H₆₆BrNO₁₂Si

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 23 ℃;
DOI:10.1016/j.tetlet.2013.06.085

Reference yield:

: 1448441-39-1
C₃₈H₆₁BrO₁₂Si

: 1448441-40-4
C₄₀H₆₆BrNO₁₂Si

Guidance literature:: Multi-step reaction with 2 steps

1: chloro-trimethyl-silane; sodium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 23 °C

With dmap; chloro-trimethyl-silane; sodium hexamethyldisilazane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2013.06.085

Reference yield:

: 55955-32-3
3-O-(β-D-galactopyranosyl)-1,2-O-isopropylidene-sn-glycerol

: 1448441-40-4
C₄₀H₆₆BrNO₁₂Si

Guidance literature:: Multi-step reaction with 9 steps

1: triethylamine; dmap / dichloromethane / 23 °C

2: camphor-10-sulfonic acid / dichloromethane / 23 °C

3: dmap; 2,6-dimethylpyridine / dichloromethane / 23 °C

4: tetrabutyl ammonium fluoride; acetic acid / N,N-dimethyl-formamide / 23 °C

5: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / benzene; water / 23 °C

6: sodium hydroxide / water; methanol / 23 °C

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 23 °C

8: chloro-trimethyl-silane; sodium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C

9: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 23 °C

With 2,6-dimethylpyridine; dmap; chloro-trimethyl-silane; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; tetra(n-butyl)ammonium hydrogensulfate; sodium hexamethyldisilazane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; benzene; 7: |Claisen-Ireland Rearrangement;
DOI:10.1016/j.tetlet.2013.06.085