Methyl phenanthro[2,3-d][1,3]dioxole-5-carboxylate

Base Information

• Chemical Name: Methyl phenanthro[2,3-d][1,3]dioxole-5-carboxylate
• CAS No.: 38288-34-5
• Molecular Formula: C₁₇H₁₂O₄
• Molecular Weight: 280.28
• NSC Number: 89117
• DSSTox Substance ID: DTXSID90293388
• Wikidata: Q82032089
• Mol file: 38288-34-5.mol

Synonyms:38288-34-5;methyl phenanthro[2,3-d][1,3]dioxole-5-carboxylate;NSC89117;NCIOpen2_005454;DTXSID90293388;NSC-89117

Chemical Property of Methyl phenanthro[2,3-d][1,3]dioxole-5-carboxylate

Chemical Property:

• Vapor Pressure: 6.42E-09mmHg at 25°C
• XLogP3: 4.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 280.07355886
• Heavy Atom Count: 21
• Complexity: 410

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC(=O)C1=CC2=CC3=C(C=C2C4=CC=CC=C41)OCO3

Technology Process of Methyl phenanthro[2,3-d][1,3]dioxole-5-carboxylate

There total 2 articles about Methyl phenanthro[2,3-d][1,3]dioxole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + phenanthro[2,3-d][1,3]dioxole-5-carboxylic acid (38288-33-4) → phenanthro[2,3-d][1,3]dioxole-5-carboxylic acid methyl ester (38288-34-5)

Guidance literature:

With sulfuric acid;

DOI:10.1021/ja01370a064

Reference yield:

→ phenanthro[2,3-d][1,3]dioxole-5-carboxylic acid methyl ester (38288-34-5)

Guidance literature:

aus der entspr. Aminosaeure, 1) Amylnitrit, 2) Ringschluss;

DOI:10.1007/BF00905427

upstream raw materials:

methanol

phenanthro[2,3-d][1,3]dioxole-5-carboxylic acid