racem.-bis-(1-phenyl-ethyl)-disulfide

Base Information

• Chemical Name: racem.-bis-(1-phenyl-ethyl)-disulfide
• CAS No.: 50999-18-3
• Molecular Formula: C₁₆H₁₈S₂
• Molecular Weight: 274.451
• Mol file: 50999-18-3.mol

Synonyms:

Chemical Property of racem.-bis-(1-phenyl-ethyl)-disulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of racem.-bis-(1-phenyl-ethyl)-disulfide

There total 6 articles about racem.-bis-(1-phenyl-ethyl)-disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R,R)-(+)-bis(1-phenylethyl) trisulfide (82916-72-1) → (R,R)-(+)-bis(1-phenylethyl) disulfide (82916-73-2) + (R,S)-meso-bis(1-phenylethyl) disulfide (50999-18-3)

Guidance literature:

With Hexamethylphosphorous triamide; In acetonitrile; Product distribution; Ambient temperature; other solvents;

DOI:10.1021/ja00386a034

Reference yield:

1-Phenylethanethiol (33877-11-1,33877-16-6,75081-57-1,6263-65-6) → racem.-bis-(1-phenyl-ethyl)-disulfide (50999-18-3,50999-19-4,52053-61-9,82916-73-2)

Guidance literature:

With ethanol; iodine;

DOI:10.1007/BF00905691

Reference yield:

(S)-1-mercapto-1-phenylethane (33877-11-1) → bis-((S)-1-phenyl-ethyl)-disulfide (50999-18-3,50999-19-4,52053-61-9,82916-73-2)

Guidance literature:

With ethanol; iodine;

upstream raw materials:

(S)-1-mercapto-1-phenylethane

1-Phenylethanethiol

bis-((S)-1-phenyl-ethyl)-disulfide

(R,R)-(+)-bis(1-phenylethyl) disulfide

Downstream raw materials:

racem.-bis-(1-phenyl-ethyl)-disulfide

(1,2-dibromoethyl)benzene

Refernces