2-Methyl-4-phenylsulfanyl-2,5-dihydrothiophene 1,1-dioxide

Base Information

Chemical Name:2-Methyl-4-phenylsulfanyl-2,5-dihydrothiophene 1,1-dioxide
CAS No.:104664-79-1
Molecular Formula:C11H12O2S2
Molecular Weight:240.347
Hs Code.:
DSSTox Substance ID:DTXSID50546908
Nikkaji Number:J1.412.096C
Mol file:104664-79-1.mol

Synonyms:104664-79-1;DTXSID50546908;2-Methyl-4-(phenylsulfanyl)-2,5-dihydro-1H-1lambda~6~-thiophene-1,1-dione

Suppliers and Price of 2-Methyl-4-phenylsulfanyl-2,5-dihydrothiophene 1,1-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methyl-4-phenylsulfanyl-2,5-dihydrothiophene 1,1-dioxide

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:240.02787197
Heavy Atom Count:15
Complexity:345

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C=C(CS1(=O)=O)SC2=CC=CC=C2

Technology Process of 2-Methyl-4-phenylsulfanyl-2,5-dihydrothiophene 1,1-dioxide

There total 3 articles about 2-Methyl-4-phenylsulfanyl-2,5-dihydrothiophene 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 930-69-8
sodium thiophenolate

: 125946-21-6
4-bromo-2-methyl-4,5-dihydrothiophene 1,1-dioxide

: 104664-79-1
2-methyl-4-(phenylthio)-2,5-dihydrothiophene 1,1-dioxide

: 104664-91-7
5-methyl-3-(phenylthio)-4,5-dihydrothiophene 1,1-dioxide

Guidance literature:: In tetrahydrofuran; for 6h; Ambient temperature;

Reference yield: 8.0%

: 930-69-8
sodium thiophenolate

: 125946-21-6
4-bromo-2-methyl-4,5-dihydrothiophene 1,1-dioxide

: 104664-79-1
2-methyl-4-(phenylthio)-2,5-dihydrothiophene 1,1-dioxide

: 104664-87-1
2-methyl-4-(phenylthio)-4,5-dihydrothiophene 1,1-dioxide

Guidance literature:: In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield:

: 61464-28-6
2-methyl-4,5-dihydrothiophene 1,1-dioxide

: 104664-79-1
2-methyl-4-(phenylthio)-2,5-dihydrothiophene 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / NBS, azobisisobutyronitrile / CCl₄ / 12 h / Heating

2: 8 percent / tetrahydrofuran / 2 h / Ambient temperature

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; tetrachloromethane;