N,N'-Dimethyl-4,4'-bis(2,3-dimethoxybenzoesaeure-methylester)

Base Information

Chemical Name:N,N'-Dimethyl-4,4'-bis(2,3-dimethoxybenzoesaeure-methylester)
CAS No.:145731-70-0
Molecular Formula:C₃₉H₄₂N₂O₁₀
Molecular Weight:698.77
Hs Code.:

N,N'-Dimethyl-4,4'-<methylenbis(1,4-phenylenmethyleniminocarbonyl)>bis(2,3-dimethoxybenzoesaeure-methylester)

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Chemical Property of N,N'-Dimethyl-4,4'-bis(2,3-dimethoxybenzoesaeure-methylester)

Chemical Property:

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Technology Process of N,N'-Dimethyl-4,4'-bis(2,3-dimethoxybenzoesaeure-methylester)

There total 2 articles about N,N'-Dimethyl-4,4'-bis(2,3-dimethoxybenzoesaeure-methylester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 110027-64-0
Bis<4-<(methylamino)methyl>phenyl>methan

: 75956-64-8
2,3-Dimethoxy-4-(methoxycarbonyl)benzoylchlorid

: 145731-70-0
N,N'-Dimethyl-4,4'-bis(2,3-dimethoxybenzoesaeure-methylester)

Guidance literature:: With triethylamine; In tetrahydrofuran; for 8h; Ambient temperature;

Reference yield:

: 16980-01-1
bis(4-bromomethylphenyl)methane

: 145731-70-0
N,N'-Dimethyl-4,4'-bis(2,3-dimethoxybenzoesaeure-methylester)

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / Na₂CO₃ / ethanol / 12 h / Ambient temperature

2: 67 percent / triethylamine / tetrahydrofuran / 8 h / Ambient temperature

With sodium carbonate; triethylamine; In tetrahydrofuran; ethanol;

Reference yield:

: 145731-70-0
N,N'-Dimethyl-4,4'-bis(2,3-dimethoxybenzoesaeure-methylester)

: 145731-74-4
C₃₇H₃₆Cl₂N₂O₈

Guidance literature:: With sodium hydroxide; thionyl chloride; Yield given. Multistep reaction; 1.) MeOH, H₂O, 90 deg C, 12 h;
DOI:10.1039/C39920001584