6-(9-Bromononyl)-2-methoxybenzoic acid

Base Information

Chemical Name:6-(9-Bromononyl)-2-methoxybenzoic acid
CAS No.:173473-50-2
Molecular Formula:C₁₇H₂₅BrO₃
Molecular Weight:357.288
Hs Code.:

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Chemical Property of 6-(9-Bromononyl)-2-methoxybenzoic acid

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Technology Process of 6-(9-Bromononyl)-2-methoxybenzoic acid

There total 7 articles about 6-(9-Bromononyl)-2-methoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 173473-49-9
6-(9-Hydroxynonyl)-2-methoxybenzoic acid

: 173473-50-2
6-(9-Bromononyl)-2-methoxybenzoic acid

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; Ambient temperature;

Reference yield:

: 2774-84-7
undec-10-yn-1-ol

: 173473-50-2
6-(9-Bromononyl)-2-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 7 steps

1: p-TsOH*H₂O / 2 h / Ambient temperature

2: n-BuLi / tetrahydrofuran; hexane

3: p-TsOH*H₂O / methanol / 1 h / Heating

4: 100 percent / pyridine / 3.5 h / Ambient temperature

5: 62 percent / dichloromaleic anhydride / 200 °C

6: 94 percent / 2 M KOH / ethanol / Heating

7: 68 percent / CBr₄, PPh₃ / CH₂Cl₂ / Ambient temperature

With pyridine; potassium hydroxide; n-butyllithium; dichloromaleic acid anhydride; carbon tetrabromide; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane;

Reference yield:

: 51953-88-9,151329-50-9
1-[(tetrahydropyran-2-yl)oxy]undec-10-yne

: 173473-50-2
6-(9-Bromononyl)-2-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: n-BuLi / tetrahydrofuran; hexane

2: p-TsOH*H₂O / methanol / 1 h / Heating

3: 100 percent / pyridine / 3.5 h / Ambient temperature

4: 62 percent / dichloromaleic anhydride / 200 °C

5: 94 percent / 2 M KOH / ethanol / Heating

6: 68 percent / CBr₄, PPh₃ / CH₂Cl₂ / Ambient temperature

With pyridine; potassium hydroxide; n-butyllithium; dichloromaleic acid anhydride; carbon tetrabromide; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane;