2,3-Piperidinedione, 3-[(4-methoxyphenyl)hydrazone]

Base Information

Chemical Name:2,3-Piperidinedione, 3-[(4-methoxyphenyl)hydrazone]
CAS No.:104742-98-5
Molecular Formula:C12H15N3O2
Molecular Weight:233.27
Hs Code.:
Mol file:104742-98-5.mol

Synonyms:2,3-Dioxo-piperidin-(4-methoxy-phenylhydrazon)-(3);piperidine-2,3-dione-3-(4-methoxy-phenylhydrazone);Piperidin-2,3-dion-3-(4-methoxy-phenylhydrazon);

Suppliers and Price of 2,3-Piperidinedione, 3-[(4-methoxyphenyl)hydrazone]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-[2-(4-METHOXYPHENYL)HYDRAZONO]PIPERIDIN-2-ONE 95.00%
5MG
$ 499.94

Total 1 raw suppliers

Chemical Property of 2,3-Piperidinedione, 3-[(4-methoxyphenyl)hydrazone]

Chemical Property:

PSA：62.72000
LogP:1.77490

Purity/Quality:

99% ^*data from raw suppliers

3-[2-(4-METHOXYPHENYL)HYDRAZONO]PIPERIDIN-2-ONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-Piperidinedione, 3-[(4-methoxyphenyl)hydrazone]

There total 7 articles about 2,3-Piperidinedione, 3-[(4-methoxyphenyl)hydrazone] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17216-62-5
diethyl 2-(2-cyanoethyl)malonate

: 104742-98-5
2,3-dioxopiperidine 3-(p-methoxyphenyl)hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Raney Ni / ethanol / 6 h / 80 °C / 58840.6 Torr

2: 1.) aq. KOH, 2.) aq. CH₃COOH / 1.) RT, overnight, 2.) 0 deg C, 4 h

With potassium hydroxide; hydrogen; acetic acid; nickel; In ethanol;
DOI:10.1021/jm00051a007

Reference yield:

: 104742-98-5
2,3-dioxopiperidine 3-(p-methoxyphenyl)hydrazone

Guidance literature:: With methanol; nickel; at 70 ℃; under 73550.8 Torr; Hydrogenation;

Reference yield:

: 41888-21-5
3-carboxy-2-piperidone

: 104-94-9
4-methoxy-aniline

: 104742-98-5
2,3-dioxopiperidine 3-(p-methoxyphenyl)hydrazone

Guidance literature:: 4-methoxy-aniline; With hydrogenchloride; sodium nitrite; at 0 ℃;

3-carboxy-2-piperidone; With acetic acid; at 0 ℃;
DOI:10.1016/j.bmc.2004.03.005