ethyl 2-ethoxycarbonyl-3-methyl-4-phenylbutanoate

Base Information Edit

Chemical Name:ethyl 2-ethoxycarbonyl-3-methyl-4-phenylbutanoate
CAS No.:34599-62-7
Molecular Formula:C₁₆H₂₂O₄
Molecular Weight:278.348
Hs Code.:
Mol file:34599-62-7.mol

Synonyms:

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Chemical Property of ethyl 2-ethoxycarbonyl-3-methyl-4-phenylbutanoate Edit

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of ethyl 2-ethoxycarbonyl-3-methyl-4-phenylbutanoate

There total 5 articles about ethyl 2-ethoxycarbonyl-3-methyl-4-phenylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1462-12-0
diethyl ethylidenemalonate

: 60-12-8
2-phenylethanol

: 34599-62-7,88383-10-2,88383-11-3
ethyl 2-ethoxycarbonyl-3-methyl-4-phenylbutanoate

Guidance literature:: With cerium(III) bromide; tetrabutylammomium bromide; In acetonitrile; at 20 ℃; for 24h; Irradiation; Sealed tube; Inert atmosphere;
DOI:10.1021/jacs.9b05932 DOI:10.1021/jacs.9b05932

Reference yield:

: 300-57-2,57807-91-7
allylbenzene

: 34599-62-7,88383-10-2,88383-11-3
ethyl 2-ethoxycarbonyl-3-methyl-4-phenylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: glacial acetic acid; HBr

2: sodium ethylate; ethanol; potassium iodide / 120 °C

With ethanol; hydrogen bromide; sodium ethanolate; acetic acid; potassium iodide;